Quantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC–MS/ MS and GC–MS/MS

Basit Öğe Kaydı
dc.authorid0000-0002-9208-9852en_US
dc.authorid0000-0003-2438-5454en_US
dc.authorid0000-0001-9701-2240en_US
dc.authorid0000-0002-0868-2769en_US
dc.contributor.authorElmastaş, Ayhan
dc.contributor.authorUmaz, Adil
dc.contributor.authorPirinç, Vedat
dc.contributor.authorAydın, Fırat
dc.date.accessioned2023-08-08T06:29:22Z
dc.date.available2023-08-08T06:29:22Z
dc.date.issued2023en_US
dc.departmentDicle Üniversitesi, Ziraat Fakültesi, Bahçe Bitkileri Bölümüen_US
dc.description.abstractPesticides are the potent agrochemicals used to successfully manage, repel, or stop pests and weeds in agricultural production. This study analyzed 222 pesticide active substances in 90 samples of seven different vegetables and fruits acquired from producers through liquid chromatography-mass spectrometry/mass spectrometry (LC–MS/MS) and gas chromatography-mass spectrometry/mass spectrometry (GC–MS/MS) technology. The validation parameters of each pesticide’s active substances were determined. The LOD, LOQ values, and recovery studies of the 222 active substances were 3.00, 10.00 ng/g, and between 76.07 and 108.08%, respectively. The correlation coefficients and measurement uncertainty were determined to be between 0.990–0.999 and 8.91– 31.46%, respectively. There were active substances of chlorpyrifos, acetamiprid, azoxystrobin, difenoconazole, malathion, dieldrin, boscalid, triticonazole, tebuconazole, triadimenol, trifloxystrobin, pirimicarb, and dodine among the vegetable and fruit samples used in the study. There were no active substances in 55 (61%) samples. Among the 35 samples (39%), 31 samples (34%) contained only one active substance, whereas four (5%) contained two active substances. However, the amount of active substances in six (7%) samples was above the maximum residue levels (MRL) limits. Various processes used in the study revealed that peeling was the most effective pesticide residue removal strategy. The washing procedure also proved that it reduced some pesticide residues but failed to eliminate all pesticides. The peeling process successfully reduced a significant amount of the active substances from the products, however, residues remained. Washing the fruits with hot water was also effective in removing residues. As a result, analyses of the peeled sections yielded higher pesticide residue concentrations than those of the entire product.en_US
dc.identifier.citationElmastaş, A., Umaz, A., Pirinç, V. ve Aydın, F. (2023). Quantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC–MS/ MS and GC–MS/MS. Environmental Monitoring and Assessment, 195(2), 195-277.en_US
dc.identifier.doi10.1007/s10661-022-10910-2
dc.identifier.endpage277en_US
dc.identifier.issn0167-6369
dc.identifier.issue2en_US
dc.identifier.pmid36609771
dc.identifier.scopus2-s2.0-85145773761
dc.identifier.scopusqualityQ2
dc.identifier.startpage195en_US
dc.identifier.urihttps://www.scopus.com/record/display.uri?eid=2-s2.0-85145773761
dc.identifier.urihttps://hdl.handle.net/11468/12447
dc.identifier.volume195en_US
dc.identifier.wosWOS:000910870000002
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorPirinç, Vedat
dc.institutionauthorAydın, Fırat
dc.language.isoenen_US
dc.publisherSpringer Science and Business Mediaen_US
dc.relation.ispartofEnvironmental Monitoring and Assessment
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectPesticidesen_US
dc.subjectVegetableen_US
dc.subjectFruiten_US
dc.subjectLC-MS/ MSen_US
dc.subjectGC-MS/MSen_US
dc.titleQuantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC–MS/ MS and GC–MS/MSen_US
dc.titleQuantitative determination and removal of pesticide residues in fresh vegetables and fruit products by LC–MS/ MS and GC–MS/MS
dc.typeArticleen_US

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
Quantitative determination and removal of pesticide residues in fresh vegetables and fruit products.pdf
Boyut:
773.13 KB
Biçim:
Adobe Portable Document Format
Açıklama:
Makale Dosyası
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Bahçe Bitkileri Bölümü Koleksiyonu
PubMed İndeksli Yayın Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu
WoS İndeksli Yayınlar Koleksiyonu