Solvent-free synthesis of chiral Schiff-base ligands based on ferrocene under microwave irradiation and application to enantioselective nitroaldol (Henry) reaction

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dc.contributor.authorÖztürk, Gülşen
dc.contributor.authorÇolak, Mehmet
dc.contributor.authorDemirel, Nadir
dc.contributor.orcid0000-0002-3774-2652
dc.contributor.orcid0000-0002-8571-5552
dc.date.accessioned2024-04-24T15:59:22Z
dc.date.available2024-04-24T15:59:22Z
dc.date.issued2011
dc.departmentDicle Üniversitesi, Fen Fakültesi, Kimya Bölümüen_US
dc.description.abstractChiral Schiff-bases 3a-f based on ferrocene were designed and synthesized using solvent-free methods by mixing ferrocene carbaldehyde 1 with amino alcohols and amines 2a-f under microwave irradiation and classical method for the enantioselective nitroaldol (Henry) reaction. The Schiff-bases were obtained in shorter reaction times and improved yield under microwave irradiation method over classical method. The highest enantioselectivity was observed in ligand 3e (95% ee) when CH2Cl2 was used as solvent. Chirality 23: 374-378, 2011. (c) 2011 Wiley-Liss, Inc.en_US
dc.identifier.citationÖztürk, G., Çolak, M. ve Demirel, N. (2011). Solvent-free synthesis of chiral Schiff-base ligands based on ferrocene under microwave irradiation and application to enantioselective nitroaldol (Henry) reaction. Chirality, 23(5), 374-378.
dc.identifier.doi10.1002/chir.20934
dc.identifier.endpage378en_US
dc.identifier.issn0899-0042
dc.identifier.issn1520-636X
dc.identifier.issue5en_US
dc.identifier.pmid21488104
dc.identifier.scopus2-s2.0-79954531846
dc.identifier.scopusqualityQ2
dc.identifier.startpage374en_US
dc.identifier.urihttps://doi.org/10.1002/chir.20934
dc.identifier.urihttps://hdl.handle.net/11468/14012
dc.identifier.urihttps://onlinelibrary.wiley.com/doi/10.1002/chir.20934
dc.identifier.volume23en_US
dc.identifier.wosWOS:000289635300002
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorÖztürk, Gülşen
dc.institutionauthorÇolak, Mehmet
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofChirality
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectFerroceneen_US
dc.subjectMicrowave irradiationen_US
dc.subjectChiral schiff-basesen_US
dc.subjectNitro aldol reactionen_US
dc.subjectHenry reactionen_US
dc.titleSolvent-free synthesis of chiral Schiff-base ligands based on ferrocene under microwave irradiation and application to enantioselective nitroaldol (Henry) reactionen_US
dc.titleSolvent-free synthesis of chiral Schiff-base ligands based on ferrocene under microwave irradiation and application to enantioselective nitroaldol (Henry) reaction
dc.typeArticleen_US

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