Preconcentrations of Zn(II) and Hg(II) in environmental and food samples by SPE on B. licheniformis loaded amberlite XAD-4

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dc.authorid0000-0001-5223-9919en_US
dc.contributor.authorÖzdemir, Sadin
dc.contributor.authorKılınç, Ersin
dc.contributor.authorAcer, Ömer
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2022-12-21T07:06:02Z
dc.date.available2022-12-21T07:06:02Z
dc.date.issued2022en_US
dc.departmentDicle Üniversitesi, Diyarbakır Teknik Bilimler Meslek Yüksekokulu, Kimya ve Kimyasal İşleme Teknolojileri Bölümüen_US
dc.description.abstractIn this work, the separations and preconcentrations of Zn(II) and Hg(II) ions on Bacillus lichenifoemis loaded onto Amberlite XAD-4 resin by solid-phase extraction has been performed. The biosorbent was characterized by using FT-IR, SEM, and EDX. pH, sample flow rate, eluent type and concentration, amount of B. licheniformis and XAD-4 resin, sample volume, and possible interfering ions effect were investigated in details as experimental variables in the SPE procedure. Limit of detection values for Zn(II) and Hg(II) were detected as 0.03 and 0.06 ng-mL(-1), respectively. 0.2-15 ng-mL(-1) linear range values were achieved for Zn(II) and Hg(II), respectively. Relative standard deviation values were found to be lower than 5%. For validation of the procedure, the certified standard reference materials (CWW-TM-D, EU-L-2, NCS ZC73O14, NCS ZC73350) were analyzed. The concentrations of Zn(II) and Hg( II) in water and food samples were measured by ICP-OES. Consequently, it can be inferred that the immobilized B. licheniformis microcolumn has ideal selectivity for Zn(II) and Hg(II) biosorption.en_US
dc.identifier.citationÖzdemir, S., Kılınç, E., Acer, Ö. ve Soylak, M. (2022). Preconcentrations of Zn(II) and Hg(II) in environmental and food samples by SPE on B. licheniformis loaded amberlite XAD-4. Biological Trace Element Research, 200(4), 1972-1980.en_US
dc.identifier.doi10.1007/s12011-021-03000-w
dc.identifier.endpage1980en_US
dc.identifier.issn0163-4984
dc.identifier.issn1559-0720
dc.identifier.issue4en_US
dc.identifier.pmid34729695
dc.identifier.scopus2-s2.0-85118450917
dc.identifier.scopusqualityQ1
dc.identifier.startpage1972en_US
dc.identifier.urihttps://link.springer.com/article/10.1007/s12011-021-03000-w
dc.identifier.urihttps://hdl.handle.net/11468/11094
dc.identifier.volume200en_US
dc.identifier.wosWOS:000713932800002
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorKılınç, Ersin
dc.language.isoenen_US
dc.publisherSpringernatureen_US
dc.relation.ispartofBiological Trace Element Research
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSolid-phase extractionen_US
dc.subjectPreconcentrationen_US
dc.subjectB. licheniformisen_US
dc.subjectZincen_US
dc.subjectMercuryen_US
dc.subjectEnvironmental samplesen_US
dc.titlePreconcentrations of Zn(II) and Hg(II) in environmental and food samples by SPE on B. licheniformis loaded amberlite XAD-4en_US
dc.titlePreconcentrations of Zn(II) and Hg(II) in environmental and food samples by SPE on B. licheniformis loaded amberlite XAD-4
dc.typeArticleen_US

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