Preconcentration and determination of copper and cadmium ions with 1,6-bis(2-carboxy aldehyde phenoxy)butane functionalized Amberlite XAD-16 by flame atomic absorption spectrometry

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dc.contributor.authorOral, Elif V.
dc.contributor.authorDolak, Ibrahim
dc.contributor.authorTemel, Hamdi
dc.contributor.authorZiyadanogullari, Berrin
dc.date.accessioned2024-04-24T16:15:07Z
dc.date.available2024-04-24T16:15:07Z
dc.date.issued2011
dc.departmentDicle Üniversitesien_US
dc.description.abstractA new chelating resin, covalently linked 1,6-bis(2-carboxy aldehyde phenoxy)butane with the Amberlite XAD-16 was synthesized and used for preconcentration of Cu(II) and Cd(II) prior to their determination by flame atomic absorption spectrometry (FAAS). It was characterized by elemental analyses and Fourier Transform Infrared Spectroscopy (FT-IR). Cu(II) and Cd(II) ions were quantitatively preconcentrated on minicolumn loaded with synthesised resin at pH 4.00 and 6.00, respectively. They were eluated with 5 mL of 0.5 mol L-1 HCl. Recoveries of Cu(II) and Cd(II) were found to be 100 +/- 2.15, 100 +/- 1.40(N= 5), the limits of detection of Cu(II) and Cd(II) in the determination by FAAS (3s, N= 20) were found to be 0.33 and 1.19 mu g L-1, respectively. The effect of foreign ions on the recovery has been investigated. The proposed method has been applied for the determination of Cu(II) and Cd(II) ions to the real samples collected from Tigris river water in Diyarbakir and Elazig cities in Turkey. Standard addition method and analysis of the certified reference material (NCS-DC 73350) was employed to check the accuracy of the method. (C) 2010 Elsevier B.V. All rights reserved.en_US
dc.identifier.doi10.1016/j.jhazmat.2010.11.048
dc.identifier.endpage730en_US
dc.identifier.issn0304-3894
dc.identifier.issn1873-3336
dc.identifier.issue1en_US
dc.identifier.pmid21159425
dc.identifier.scopus2-s2.0-79551525025
dc.identifier.scopusqualityQ1
dc.identifier.startpage724en_US
dc.identifier.urihttps://doi.org/10.1016/j.jhazmat.2010.11.048
dc.identifier.urihttps://hdl.handle.net/11468/15657
dc.identifier.volume186en_US
dc.identifier.wosWOS:000288102400091
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Hazardous Materials
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSolid Phase Extractionen_US
dc.subjectAmberlite Xad 16en_US
dc.subjectPreconcentrationen_US
dc.subjectCopperen_US
dc.subjectCadmiumen_US
dc.titlePreconcentration and determination of copper and cadmium ions with 1,6-bis(2-carboxy aldehyde phenoxy)butane functionalized Amberlite XAD-16 by flame atomic absorption spectrometryen_US
dc.titlePreconcentration and determination of copper and cadmium ions with 1,6-bis(2-carboxy aldehyde phenoxy)butane functionalized Amberlite XAD-16 by flame atomic absorption spectrometry
dc.typeArticleen_US

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