Synthesis, spectroscopic and electrochemical investigations of two vic-dioximes and their mononuclear Ni(II), Cu(II) and Co(II) metal complexes containing morpholine group

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dc.contributor.authorKılıç, Ahmet
dc.contributor.authorTaş, Eşref
dc.contributor.authorGümgüm, Bahattin
dc.contributor.authorYımaz, İsmail
dc.contributor.orcid0000-0001-9073-4339
dc.contributor.orcid0000-0002-5046-7456
dc.date.accessioned2024-04-24T15:59:22Z
dc.date.available2024-04-24T15:59:22Z
dc.date.issued2006
dc.departmentDicle Üniversitesi, Fen Fakültesi, Kimya Bölümüen_US
dc.description.abstractTwo vic-dioxime ligands (LxH2) containing morpholine group have been synthesized from 4-[2-(dimethylaminoethyl)] morpholine with anti-phenylchloroglyoxime or anti-monochloroglyoxime in absolute THF at -15 degrees C. Reaction of two vic-dioxime ligands with MCl2 center dot nH(2)O (M: Ni, Cu or Co and n=2 or 6) salts in 1 : 2 molar ratio afforded metal complexes of type [M(LxH)(2)] or [M(LxH)(2)center dot 2H(2)O]. All of metal complexes are non-electrolytes as shown by their molar conductivities (Lambda(m)) in DMF (dimethyl formamide) at 10(-3) mol.L-1. Structures of the ligands and metal complexes have been solved by elemental analyses, FT-IR, UV-Vis, H-1 NMR and C-13 NMR, magnetic susceptibility measurements, molar conductivity measurements. Furthermore, redox properties of the metal complexes were investigated by cyclic voltammetry.en_US
dc.identifier.citationKılıç, A., Taş, E., Gümgüm, B. ve Yımaz, İ. (2006). Synthesis, spectroscopic and electrochemical investigations of two vic-dioximes and their mononuclear Ni(II), Cu(II) and Co(II) metal complexes containing morpholine group. Chinese Journal of Chemistry, 24(11), 1599-1604.
dc.identifier.doi10.1002/cjoc.200690299
dc.identifier.endpage1604en_US
dc.identifier.issn1001-604X
dc.identifier.issn1614-7065
dc.identifier.issue11en_US
dc.identifier.scopus2-s2.0-33750936898
dc.identifier.scopusqualityQ1
dc.identifier.startpage1599en_US
dc.identifier.urihttps://doi.org/10.1002/cjoc.200690299
dc.identifier.urihttps://hdl.handle.net/11468/14018
dc.identifier.urihttps://onlinelibrary.wiley.com/doi/10.1002/cjoc.200690299
dc.identifier.volume24en_US
dc.identifier.wosWOS:000242009000018
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorGümgüm, Bahattin
dc.language.isoenen_US
dc.publisherWiley-V C H Verlag Gmbhen_US
dc.relation.ispartofChinese Journal of Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectMorpholineen_US
dc.subjectElectrochemistryen_US
dc.subjectDioximeen_US
dc.subjectStructureen_US
dc.subjectMetal complexen_US
dc.subjectCyclic voltammetryen_US
dc.titleSynthesis, spectroscopic and electrochemical investigations of two vic-dioximes and their mononuclear Ni(II), Cu(II) and Co(II) metal complexes containing morpholine groupen_US
dc.titleSynthesis, spectroscopic and electrochemical investigations of two vic-dioximes and their mononuclear Ni(II), Cu(II) and Co(II) metal complexes containing morpholine group
dc.typeArticleen_US

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