A sensitive determination of Brilliant Blue FCF in some food samples using hydrophillic deep eutectic solvent-assisted magnetic nano gel-based dispersive solid phase microextraction prior to spectrophotometric analysis

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dc.authorid0000-0002-2861-5504en_US
dc.authorid0000-0001-8522-6620en_US
dc.contributor.authorErek, Figen
dc.contributor.authorLanjwani, Muhammad Farooque
dc.contributor.authorTüzen, Mustafa
dc.date.accessioned2024-06-24T08:25:13Z
dc.date.available2024-06-24T08:25:13Z
dc.date.issued2024en_US
dc.departmentDicle Üniversitesi, Fen Fakültesi, Kimya Bölümüen_US
dc.description.abstractA new magnetic nano gel (MNG) was prepared from choline chloride/phenol deep eutectic solvent and magnetic amberlite XAD-7 nanocomposite. The dispersive solid phase micro extraction (dSPME) method was developed for seperation and preconcentration of Brilliant Blue FCF (BB) by the prepared MNG. In this study, firstly, the optimum DES type and mole ratio of DES were investigated before response surface methodology optimization. Then, the effect of the MNG-dSPME experimental parameters were optimized by response surface methodology using central composite design. Under the optimum microextraction conditions, limit of detection (LOD), limit of quantification (LOQ), preconcentration factor (PF), enhencament factor (EF) were found to be 1.15 μg L−1,3.80 µg L-1, 70, and 88, respectively. It was seen that the recovery of real samples were obtained from 95.5 to 103.6%. The pesent method was succesfully for extraction of BB in some food, personal care samples, to the best of our knowledge, this is the first study that is presented method on determination of BB by preconcentration with magnetic nano gel. The obtained results showed that the present procedure is effective, sensitive, and has high accuracy for the quantitative detection of BB.en_US
dc.identifier.citationErek, F., Lanjwani, M.F. ve Tüzen, M. (2024). A sensitive determination of Brilliant Blue FCF in some food samples using hydrophillic deep eutectic solvent-assisted magnetic nano gel-based dispersive solid phase microextraction prior to spectrophotometric analysis. Food Chemistry, 453, 1-9.en_US
dc.identifier.endpage9en_US
dc.identifier.issn0308-8146
dc.identifier.pmid38754352
dc.identifier.scopus2-s2.0-85192761807
dc.identifier.scopusqualityQ1
dc.identifier.startpage1en_US
dc.identifier.urihttps://www.sciencedirect.com/science/article/pii/S0308814624012822?via%3Dihub
dc.identifier.urihttps://hdl.handle.net/11468/28674
dc.identifier.volume453en_US
dc.identifier.wosWOS:001226817000001
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakPubMed
dc.indekslendigikaynakScopus
dc.institutionauthorErek, Figen
dc.language.isoenen_US
dc.publisherElsevier Ltden_US
dc.relation.ispartofFood Chemistry
dc.relation.isversionof10.1016/j.foodchem.2024.139632en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCentral composite designen_US
dc.subjectExperimental optimization designen_US
dc.subjectNanofluiden_US
dc.subjectPreconcentrationen_US
dc.subjectValidationen_US
dc.titleA sensitive determination of Brilliant Blue FCF in some food samples using hydrophillic deep eutectic solvent-assisted magnetic nano gel-based dispersive solid phase microextraction prior to spectrophotometric analysisen_US
dc.titleA sensitive determination of Brilliant Blue FCF in some food samples using hydrophillic deep eutectic solvent-assisted magnetic nano gel-based dispersive solid phase microextraction prior to spectrophotometric analysis
dc.typeArticleen_US

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