Crystal structure of 2-[(3S, 4S)-4-(anthracen-9-yl)-1-(4-methoxyphenyl)-2-oxoazetidin-3-yl]-2-aza-2H-phenalene-1,3-dione unknown solvate

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dc.contributor.authorCelik, Ismail
dc.contributor.authorAkkurt, Mehmet
dc.contributor.authorJarrahpour, Aliasghar
dc.contributor.authorRad, Javad Ameri
dc.contributor.authorCelik, Omer
dc.date.accessioned2024-04-24T17:08:42Z
dc.date.available2024-04-24T17:08:42Z
dc.date.issued2015
dc.departmentDicle Üniversitesien_US
dc.description.abstractThe central beta-lactam ring of the title compound, C36H24N2O4, is almost planar (r.m.s. deviation = 0.003 angstrom) and makes dihedral angles of 17.17 (19), 89.76 (17) and 78.44 (17)degrees with the benzene ring, the anthracene ring (r.m.s. deviation = 0.003 angstrom) and the 1H-benzo[de] isoquinoline-1,3(2H)-dione moiety, which is nearly planar [maximum deviation = 0.098 (2) angstrom], respectively. The molecular structure is stabilized by an intramolecular C-H center dot center dot center dot N hydrogen bond. In the crystal, molecules are linked via C-H center dot center dot center dot pi and pi-pi stacking interactions [centroid-centroid distances = 3.5270 (19) and 3.779 (2) angstrom], forming a three-dimensional structure. A region of disordered electron density, probably disordered solvent molecules, was treated with the SQUEEZE procedure in PLATON [Spek (2015). Acta Cryst. C71, 9-18], which indicated a solvent cavity of 322 angstrom(3) containing approximately 91 electrons. Their formula mass and unit-cell characteristics were not taken into account during the refinement.en_US
dc.identifier.doi10.1107/S2056989015002959
dc.identifier.endpage+en_US
dc.identifier.issn2056-9890
dc.identifier.pmid25844239
dc.identifier.scopus2-s2.0-84928108008
dc.identifier.scopusqualityQ3
dc.identifier.startpageO184en_US
dc.identifier.urihttps://doi.org/10.1107/S2056989015002959
dc.identifier.urihttps://hdl.handle.net/11468/17430
dc.identifier.volume71en_US
dc.identifier.wosWOS:000369973400038
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoenen_US
dc.publisherInt Union Crystallographyen_US
dc.relation.ispartofActa Crystallographica Section E-Crystallographic Communications
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectCrystal Structureen_US
dc.subjectBeta-Lactam Ringen_US
dc.subject2-Azetidinoneen_US
dc.subjectAnthraceneen_US
dc.subjectIntramolecular C-H Center Dot Center Dot Center Dot N Hydrogen Bonden_US
dc.subjectC-H Center Dot Center Dot Center Dot Pi Interactionsen_US
dc.subjectPi-Pi Stacking Interactionsen_US
dc.titleCrystal structure of 2-[(3S, 4S)-4-(anthracen-9-yl)-1-(4-methoxyphenyl)-2-oxoazetidin-3-yl]-2-aza-2H-phenalene-1,3-dione unknown solvateen_US
dc.titleCrystal structure of 2-[(3S, 4S)-4-(anthracen-9-yl)-1-(4-methoxyphenyl)-2-oxoazetidin-3-yl]-2-aza-2H-phenalene-1,3-dione unknown solvate
dc.typeArticleen_US

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