400-MHz nuclear magnetic resonance metabolite profiles of jaw cysts, jaw abscesses, saliva, and urine obtained by massive D2O dilution of samples

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dc.authorid0000-0002-7794-1744en_US
dc.authorid0000-0002-5471-555Xen_US
dc.authorid0000-0002-3540-8204en_US
dc.contributor.authorYılmaz, Utku Nezih
dc.contributor.authorYılmaz, Berivan Dündar
dc.contributor.authorKöylü, Mehmet Zafer
dc.date.accessioned2023-09-26T13:24:28Z
dc.date.available2023-09-26T13:24:28Z
dc.date.issued2023en_US
dc.departmentDicle Üniversitesi, Diş Hekimliği Fakültesi, Ağız-Diş-Çene Hastalıkları ve Cerrahisi Bölümüen_US
dc.description.abstractThe metabolite profiles of various cysts and abscesses outside the jaw area have been investigated by magnetic resonance spectroscopy (MRS) using water-suppression techniques. However, metabolite profiles of jaw cysts, jaw abscesses, saliva, and urine have not yet been obtained by MRS using massive D2O dilution of samples. This study was aimed at obtaining metabolite profi les of these bio-fluids by MRS without water suppression. In total, 37 jaw cysts, 19 jaw abscesses, 10 saliva, and 10 urine samples were collected. Dilutions were prepared by adding 0.06 mL of each sample to 0.94 mL D2O. Single-pulse experiments were performed using a 400 MHz nuclear magnetic resonance (NMR) spectrometer. High-resolution metabolite profiles were obtained for most jaw abscesses (13), some jaw cysts (8), all saliva, and all urine samples. Except for one jaw cyst, the remaining samples showed a broad envelope containing various metabolites. However, high-resolution spectra for these cystic fluid samples were obtained through 40% dilution with H2O. In conclusion, to the best of our knowledge, metabolite profiles of jaw cysts, abscesses, saliva, and urine by massive D2O dilution were first presented here. The presented approach does not require water suppression and uses a relatively low-frequency NMR. It is also a simple and novel method of eliminating radiation damping, reducing experimental time, and allowing relaxation measurements.en_US
dc.identifier.citationYılmaz, U. N., Yılmaz, B. D. ve Köylü, M. Z. (2023). 400-MHz nuclear magnetic resonance metabolite profiles of jaw cysts, jaw abscesses, saliva, and urine obtained by massive D2O dilution of samples. Journal of Applied Spectroscopy, 89(6), 1100-1106.en_US
dc.identifier.doi10.1007/s10812-023-01473-2
dc.identifier.endpage1106en_US
dc.identifier.issn0021-9037
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-85146848258
dc.identifier.scopusqualityQ4
dc.identifier.startpage1100en_US
dc.identifier.urihttps://link.springer.com/article/10.1007/s10812-023-01473-2
dc.identifier.urihttps://hdl.handle.net/11468/12609
dc.identifier.volume89en_US
dc.identifier.wosWOS:000920617000008
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorYılmaz, Utku Nezih
dc.institutionauthorYılmaz, Berivan Dündar
dc.institutionauthorKöylü, Mehmet Zafer
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofJournal of Applied Spectroscopy
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectJaw cysten_US
dc.subjectJaw abscessen_US
dc.subject400-MHz nuclear magnetic resonanceen_US
dc.subjectD2Oen_US
dc.subjectSalivaen_US
dc.subjectUrineen_US
dc.subjectMetabolitesen_US
dc.title400-MHz nuclear magnetic resonance metabolite profiles of jaw cysts, jaw abscesses, saliva, and urine obtained by massive D2O dilution of samplesen_US
dc.title400-MHz nuclear magnetic resonance metabolite profiles of jaw cysts, jaw abscesses, saliva, and urine obtained by massive D2O dilution of samples
dc.typeArticleen_US

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