Microwave Digestion Followed by ICP-OES for the Determination of Al, Cd, Cr, Cu, Fe, Ni, Pb, and Sn in Maize

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dc.contributor.authorDuz, M. Zahir
dc.contributor.authorCelik, K. Serdar
dc.contributor.authorAydin, Isil
dc.contributor.authorErdogan, Sait
dc.contributor.authorAydin, Firat
dc.contributor.authorHamamci, Candan
dc.date.accessioned2024-04-24T17:24:44Z
dc.date.available2024-04-24T17:24:44Z
dc.date.issued2012
dc.departmentDicle Üniversitesien_US
dc.description.abstractMaize (Zea mays L.) is currently the most widely grown crop in the world and is used not only for food and animal feed but also to produce industrial starches, biodiesel, ethanol, and oils. The present work reports the results obtained by the proposed method for the determination of metals (M, Cd, Cr, Cu, Fe, Ni, Pb and Sn) in maize by ICP-OES, using digestion with an oxidant mixture in a closed-vessel microwave oven. The results in the maize samples (minimum-maximum in mg/kg) were: Al 6.678-7.051, Sn 2.092-3.977, Cr 0.394-0.423, Cu 21.56-24.78, Fe 93.37-102.86, Ni 1.679-1.877 and Pb 0.375-0.392. The concentration of Cd was below the detection limit (< 0.03 mg/kg). The certified reference material, CRM NIST1573a Tomato Leaves, was used in order to verify the accuracy of the microwave digestion method. The results of this study were in good agreement with the certified values.en_US
dc.identifier.doi10.46770/AS.2012.03.002
dc.identifier.endpage82en_US
dc.identifier.issn0195-5373
dc.identifier.issn2708-521X
dc.identifier.issue3en_US
dc.identifier.scopus2-s2.0-84864402756en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpage78en_US
dc.identifier.urihttps://doi.org/10.46770/AS.2012.03.002
dc.identifier.urihttps://hdl.handle.net/11468/19809
dc.identifier.volume33en_US
dc.identifier.wosWOS:000306720800002
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherAtomic Spectroscopy Press Ltden_US
dc.relation.ispartofAtomic Spectroscopyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subject[No Keyword]en_US
dc.titleMicrowave Digestion Followed by ICP-OES for the Determination of Al, Cd, Cr, Cu, Fe, Ni, Pb, and Sn in Maizeen_US
dc.typeArticleen_US

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