New voltammetric approach to the quantitative estimation of sildenafil citrate in tablets using disposable pencil graphite electrode
dc.contributor.author | Güzel, Remziye | |
dc.contributor.author | Ekşi, Haslet | |
dc.contributor.author | Dinç, Erdal | |
dc.contributor.author | Solak, Ali Osman | |
dc.date.accessioned | 2024-04-24T17:56:32Z | |
dc.date.available | 2024-04-24T17:56:32Z | |
dc.date.issued | 2014 | |
dc.department | Dicle Üniversitesi, Ziya Gökalp Eğitim Fakültesi, Matematik ve Fen Bilimleri Eğitimi Bölümü | en_US |
dc.description.abstract | The voltammetric behavior of sildenafil citrate (SC) was studied through differential pulse stripping voltammetry. The best sensitivity, optimal experimental conditions and settings for the voltammetric method development were obtained by applying experimental design and optimization methodology to the designed sample runs at different accumulation times, accumulation potentials and pHs. The linearity over the concentration range 1 × 10-7 M-8 × 10-6 M for SC was determined and the limit of detection (LOD) was 3.1 × 10-8 M. For the method ability and validity, mean recovery result and relative standard deviation were found to be 99.3% and 2.19%, respectively. The method was applied to the determination of SC in pharmaceutical and plasma samples. | en_US |
dc.identifier.citation | Güzel, R., Ekşi, H., Dinç, E. ve Solak, A. O. (2014). New voltammetric approach to the quantitative estimation of sildenafil citrate in tablets using disposable pencil graphite electrode. Sensor Letters, 12(11), 1675-1681. | |
dc.identifier.doi | 10.1166/sl.2014.3384 | |
dc.identifier.endpage | 1681 | en_US |
dc.identifier.issn | 1546-198X | |
dc.identifier.issue | 11 | en_US |
dc.identifier.scopus | 2-s2.0-84919359988 | en_US |
dc.identifier.scopusquality | N/A | en_US |
dc.identifier.startpage | 1675 | en_US |
dc.identifier.uri | https://doi.org/10.1166/sl.2014.3384 | |
dc.identifier.uri | https://hdl.handle.net/11468/23558 | |
dc.identifier.volume | 12 | en_US |
dc.indekslendigikaynak | Scopus | |
dc.language.iso | en | en_US |
dc.publisher | American Scientific Publishers | en_US |
dc.relation.ispartof | Sensor Letters | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Differential pulse stripping voltammetric determination | en_US |
dc.subject | Experimental design and optimization | en_US |
dc.subject | Pencil graphite electrode | en_US |
dc.subject | Plasma samples | en_US |
dc.subject | Sildenafil citrate | en_US |
dc.title | New voltammetric approach to the quantitative estimation of sildenafil citrate in tablets using disposable pencil graphite electrode | en_US |
dc.type | Article | en_US |