A novel magnetized bio-solid phase extractor for the preconcentrations of Hg(II), Ni(II) and Zn(II) from foods
Yükleniyor...
Tarih
2024
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Academic Press Inc.
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
Herein, Agaricus augustus, a mushroom, loaded on γ-Fe2O3 magnetic nanoparticles was developed as a biosorbent for the simultaneous preconcentrations of trace levels of Hg(II), Ni(II), and Zn(II)) in tap water, beverages, and some food samples prior to their determination by inductively coupled plasma optical emission spectrometry (ICP-OES). The experimental factors affecting the extraction performance were carefully examined throughout the investigation. The best experimental conditions were determined as pH 4.0, 3 mL/min of sample flow rate, 75 mg of biosorbent, 100 mg of γ-Fe2O3 magnetic nanoparticles, and 500 mL of sample volume. LOD values were determined as 0.016, 0.011, and 0.023 ng/mL, respectively for Hg(II), Ni(II), and Zn(II). The biosorption capacities were determined as 47.2 mg/g for Hg(II), 51.5 mg/g for Ni(II), and 49.0 mg/g for Zn(II). The effectiveness of the recommended method was assessed using certified reference material.
Açıklama
Anahtar Kelimeler
Agaricus augustus, Biosorbent, Magnetic solid phase extraction, Preconcentration, Trace metals, γ-Fe2O3 - Agaricus augustus
Kaynak
Journal of Food Composition and Analysis
WoS Q Değeri
Q2
Scopus Q Değeri
Q1
Cilt
134
Sayı
Künye
Yalçın, M. S., Özdemir, S., Kılınç, E. ve Soylak, M. (2024). A novel magnetized bio-solid phase extractor for the preconcentrations of Hg(II), Ni(II) and Zn(II) from foods. Journal of Food Composition and Analysis, 134, 1-8.
