Solid-phase extraction of copper as 1-(2-pyridylazo)-2-naphthol (PAN) chelates on Coprinus atramentaria

Basit Öğe Kaydı
dc.contributor.authorErbas, Zeliha
dc.contributor.authorMaulana, Rizqan
dc.contributor.authorYilmaz, Erkan
dc.contributor.authorOzdemir, Sadin
dc.contributor.authorKilinc, Ersin
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2024-04-24T16:24:34Z
dc.date.available2024-04-24T16:24:34Z
dc.date.issued2020
dc.departmentDicle Üniversitesien_US
dc.description.abstractA solid-phase extraction method for separation-preconcentration of copper as 1-(2-pyridylazo)-2-naphthol (PAN) on Coprinus atramentaria has been presented. The copper concentration was determined by micro-sampling flame atomic absorption spectrometry (FAAS). It could be discussed that the developed method has low LOD in addition to high preconcentration factor. By considering the over advantages of recommended method, we can suggest the use of its to preconcentration of Cu(II) by routinly. The various analytical factors affecting the efficiency of extraction were optimised. Copper(II)-PAN chelate was quantitatively recovered at pH 6.0 on Coprinus atramentaria and eluted with 2 M HNO3. The limit of detection, limit of quantification, inter-day and intra-day precision values of copper were 0.7 mu g L-1, 2.33 mu g L-1, 5.31% and 5.15%, respectively. The pre-concentration factor was 70. The method was confirmed by applying the method to certified reference materials and addition-recovery tests prior to application to the determination of copper ions in various samples recovery results. The solid-phase extraction with FAAS is a successful method for the determination of copper in different samples.en_US
dc.identifier.doi10.1080/03067319.2019.1646737
dc.identifier.endpage1003en_US
dc.identifier.issn0306-7319
dc.identifier.issn1029-0397
dc.identifier.issue9en_US
dc.identifier.scopus2-s2.0-85085731261
dc.identifier.scopusqualityQ1
dc.identifier.startpage992en_US
dc.identifier.urihttps://doi.org/10.1080/03067319.2019.1646737
dc.identifier.urihttps://hdl.handle.net/11468/16772
dc.identifier.volume100en_US
dc.identifier.wosWOS:000479479600001
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofInternational Journal of Environmental Analytical Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectPreconcentrationen_US
dc.subjectCoprinus Atramentariaen_US
dc.subjectSolid Phase Extractionen_US
dc.subjectCu(Ii)en_US
dc.subject1-(2-Pyridylazo)-2-Naphthol (Pan)en_US
dc.subjectAtomic Absorption Spectrometryen_US
dc.titleSolid-phase extraction of copper as 1-(2-pyridylazo)-2-naphthol (PAN) chelates on Coprinus atramentariaen_US
dc.titleSolid-phase extraction of copper as 1-(2-pyridylazo)-2-naphthol (PAN) chelates on Coprinus atramentaria
dc.typeArticleen_US

Dosyalar

Koleksiyon

WoS İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu