Synthesis of R-(-)-2-ethyl-N-benzyl (benzo-monoaza-15-crown-5) and the crystal structure of its sodium perchlorate complex

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dc.contributor.authorÖzbey, S
dc.contributor.authorKaynak, FB
dc.contributor.authorTogrul, M
dc.contributor.authorDemirel, N
dc.contributor.authorHosgören, H
dc.date.accessioned2024-04-24T16:19:10Z
dc.date.available2024-04-24T16:19:10Z
dc.date.issued2003
dc.departmentDicle Üniversitesien_US
dc.description.abstractA new complex of a chiral monoaza-crown ether, [R-(-)-2-ethyl-N-benzyl-4,7,10,13-tetraoxa-8,9-benzo-1-azacyclopentadec-8-ene.NaClO4], has been prepared and studied by x-ray diffraction. The compound crystallizes in space group P2(1) with cell dimensions a = 8.721(1), b = 16.318(2), c = 8.905( 1) Angstrom, beta = 100.80(1)degrees. The sodium cation is heptacoordinated and located significantly out of the best plane of the macrocycle ring. The donor atoms of the macrocycle are in the half-chair arrangement.en_US
dc.identifier.doi10.1023/A:1023042119365
dc.identifier.endpage128en_US
dc.identifier.issn1388-3127
dc.identifier.issn1573-1111
dc.identifier.issue1-2en_US
dc.identifier.scopus2-s2.0-0344596754
dc.identifier.scopusqualityQ2
dc.identifier.startpage123en_US
dc.identifier.urihttps://doi.org/10.1023/A:1023042119365
dc.identifier.urihttps://hdl.handle.net/11468/16420
dc.identifier.volume45en_US
dc.identifier.wosWOS:000182006000019
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofJournal of Inclusion Phenomena and Macrocyclic Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectBenzo-Monoaza-15-Crown-5en_US
dc.subjectChiral Crown Etheren_US
dc.subjectCrystal Structureen_US
dc.subjectSodium Complexen_US
dc.titleSynthesis of R-(-)-2-ethyl-N-benzyl (benzo-monoaza-15-crown-5) and the crystal structure of its sodium perchlorate complexen_US
dc.titleSynthesis of R-(-)-2-ethyl-N-benzyl (benzo-monoaza-15-crown-5) and the crystal structure of its sodium perchlorate complex
dc.typeArticleen_US

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