Microwave irradiation technique for synthesis of dialkyl dithiophosphoric acids

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dc.contributor.authorGümgüm, B
dc.contributor.authorBiricik, N
dc.contributor.authorBaysal, A
dc.date.accessioned2024-04-24T16:24:52Z
dc.date.available2024-04-24T16:24:52Z
dc.date.issued2002
dc.departmentDicle Üniversitesien_US
dc.description.abstractMicrowave heating technique was applied to the preparation of dialkyl dithiophosphoric acids from the reaction of alcohol with phosphorus pentasulphide. A microwave oven (CEM-MDS 2000) was utilized to determine the preparation conditions for the best yield of dialkyl dithiophosphoric acids under atmospheric pressure at various times and power Six different (C-4-C-9) chain-length of dialkyl dithiophosphoric acids were studied. All experiments were performed in an open Teflon (poly-tetrafluoroethylene) vessel. The results obtained showed that the reaction of dialkyl dithiophosphoric acids can be achieved more rapidly using microwave heating than using conventional procedures.en_US
dc.identifier.doi10.1080/10426500214305
dc.identifier.endpage2512en_US
dc.identifier.issn1042-6507
dc.identifier.issn1563-5325
dc.identifier.issue10en_US
dc.identifier.scopus2-s2.0-0036811756en_US
dc.identifier.scopusqualityQ4en_US
dc.identifier.startpage2507en_US
dc.identifier.urihttps://doi.org/10.1080/10426500214305
dc.identifier.urihttps://hdl.handle.net/11468/16880
dc.identifier.volume177en_US
dc.identifier.wosWOS:000179075500031
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofPhosphorus Sulfur and Silicon and The Related Elementsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDialkyl Dithiophosphoric Acidsen_US
dc.subjectMicrowave Irradiationen_US
dc.subjectSynthesisen_US
dc.titleMicrowave irradiation technique for synthesis of dialkyl dithiophosphoric acidsen_US
dc.typeArticleen_US

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