SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF NOVEL ARYL-DITHIOFLUOROPHOSPHONATE DERIVATIVES AND X-RAY STUDIES OF [(4-CH3OC6H4)(F)P(S)S-][PH4P+]

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dc.contributor.authorSaglam, Ertugrul Gazi
dc.contributor.authorCelik, Omer
dc.contributor.authorYilmaz, Hamza
dc.contributor.authorAcar, Nurcan
dc.date.accessioned2024-04-24T16:24:52Z
dc.date.available2024-04-24T16:24:52Z
dc.date.issued2012
dc.departmentDicle Üniversitesien_US
dc.description.abstractPotassium and tetraphenylphosphonium salts of novel aryldithiofluorophosphonic acids were synthesized. Lawesson's Reagent was allowed to react with KF in acetonitrile to yield the potassium salt of p-methoxyphenyldithiofluorophosphonic acid. Treatment of the latter with tetraphenylphosphonium chloride resulted in the formation of the tetraphenylphosphonium salt. The structures of the compounds were elucidated by FTIR, H-1, C-13, F-19, and P-31 NMR spectroscopy as well as by ESI-mass spectrometry. The molecular and crystal structure of the tetraphenylphosphonium salt, determined by single crystal X-ray diffraction, is also presented. Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the free supplemental file.en_US
dc.description.sponsorshipTechnical Research Council of Turkey (TUBITAK) [TBAG 110T016]; Ankara Universityen_US
dc.description.sponsorshipThe authors gratefully acknowledge the financial assistance of Technical Research Council of Turkey (grant number TBAG 110T016, TUBITAK) and Ankara University Research and Development Fund.en_US
dc.identifier.doi10.1080/10426507.2012.685667
dc.identifier.endpage1346en_US
dc.identifier.issn1042-6507
dc.identifier.issn1563-5325
dc.identifier.issue11en_US
dc.identifier.scopus2-s2.0-84864994552
dc.identifier.scopusqualityQ3
dc.identifier.startpage1339en_US
dc.identifier.urihttps://doi.org/10.1080/10426507.2012.685667
dc.identifier.urihttps://hdl.handle.net/11468/16881
dc.identifier.volume187en_US
dc.identifier.wosWOS:000307942300009
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherTaylor & Francis Ltden_US
dc.relation.ispartofPhosphorus Sulfur and Silicon and The Related Elements
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDithiophosphonic Aciden_US
dc.subjectPhosphonodithioic Aciden_US
dc.subjectDithiofluorophosphonic Aciden_US
dc.subjectDithiofluorophosphonateen_US
dc.subjectLawesson's Reagenten_US
dc.subjectX-Ray Structure Determinationen_US
dc.titleSYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF NOVEL ARYL-DITHIOFLUOROPHOSPHONATE DERIVATIVES AND X-RAY STUDIES OF [(4-CH3OC6H4)(F)P(S)S-][PH4P+]en_US
dc.titleSYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF NOVEL ARYL-DITHIOFLUOROPHOSPHONATE DERIVATIVES AND X-RAY STUDIES OF [(4-CH3OC6H4)(F)P(S)S-][PH4P+]
dc.typeArticleen_US

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