Synthesis and characterization of Na+, K+, Ca2+, Ba2+, Sr2+, and Pb2+ complexes with some lipophilic diaza-18-crown-6 derivatives

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dc.contributor.authorTemel, H
dc.contributor.authorHosgören, H
dc.contributor.authorBoybay, M
dc.date.accessioned2024-04-24T17:07:57Z
dc.date.available2024-04-24T17:07:57Z
dc.date.issued2002
dc.departmentDicle Üniversitesien_US
dc.description.abstractIn this study, the complexes of 7,16-Dibenzyl-4,7,10,13-tetraoxa-7,16-diazacyclooctadecane; 7,16-Dihexzyl-4,7,10,13tetraoxa-7,16-diazacyclooctadecane; 7,16-Diheptyl-4,7,10,13tetraoxa-7,16-diazacyclooctadecane; 7,16-Dioctyl-4,7,10,13tetraoxa-7,16-diazacyclooctadecane; 7,16-Dinonyl-4,7,10,13tetraoxa-7,16-diazacyclooctadecane; 7,16-Didodecyl 4,7,10, 13-tetraoxa-7,16-diazacyclooctadecane with Na+, K+, Ca2+, Ba2+, Sr2+ and Pb2+ were prepared by using perchlorates salts. Their complexes were produced by adding the solution of metal salts in ethyl alcohol to the solution of ligand in ethyl alcohol. The complexes obtained were filtered and washed with ethyl alcohol and recrystallizied in ethyl alcohol and dried in vacuum. Their complexes were investigated by using Elemental Analysis, and infrared (IR). Observed H-1 NMR,C-13 NMR, and C-13 chemical shifts are discussed in terms of conformational changes of the macrocycle.en_US
dc.identifier.doi10.1081/SL-120013128
dc.identifier.endpage8en_US
dc.identifier.issn0038-7010
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-85010749661
dc.identifier.scopusqualityQ3
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1081/SL-120013128
dc.identifier.urihttps://hdl.handle.net/11468/17112
dc.identifier.volume35en_US
dc.identifier.wosWOS:000174236000001
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherMarcel Dekker Incen_US
dc.relation.ispartofSpectroscopy Letters
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectIren_US
dc.subjectH-1/C-13 Nmr Diazamacrocyclesen_US
dc.subjectMetal Complexesen_US
dc.titleSynthesis and characterization of Na+, K+, Ca2+, Ba2+, Sr2+, and Pb2+ complexes with some lipophilic diaza-18-crown-6 derivativesen_US
dc.titleSynthesis and characterization of Na+, K+, Ca2+, Ba2+, Sr2+, and Pb2+ complexes with some lipophilic diaza-18-crown-6 derivatives
dc.typeArticleen_US

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