A new preconcentration method for the determination of pb and ni in real samples by using amberlite xad-16 functionalized with 1,6-bis(2-carboxy aldehyde phenoxy)butane

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dc.contributor.authorOral E.V.
dc.contributor.authorErdogan S.
dc.contributor.authorTemel H.
dc.contributor.authorZiyadanogullari B.
dc.contributor.authorZiyadanogullari R.
dc.date.accessioned2024-04-24T18:46:18Z
dc.date.available2024-04-24T18:46:18Z
dc.date.issued2019
dc.departmentDicle Üniversitesien_US
dc.description.abstractIn this study, a steady chelating resin matrix was formed by tying 1,6-bis(2-carboxy aldehyde phenoxy) butane to Amberlite XAD-16 resin by a-C=N-group. This synthesized adsorbent was placed into a minicolumn to separate and preconcentrate the lead and nickel ions before their determination by flame atomic absorption spectrometry (FAAS). The effects of many parameters on the preconcentration method were examined. The optimal pH value for the quantitative absorption of lead and nickel was pH 5.0. The percentage of recovery for lead and nickel was 99 ± 1.15% and 100 ± 2.70%, respectively. The detection limits of lead and nickel utilizing FAAS (3s, N= 20) were 1.47 and 1.16 µg/L, respectively. The effects of some matrix components on the recovery were analyzed. The suggested method was utilizied to determine lead and nickel in real water samples obtained from the River Tigris in Turkey, as well as in automobile exhaust particles, Romaine lettuce, and parsley. The accuracy of the proposed method was verified by using the standard addition method and the standard reference material NCS-DC 73350 Poplar Leaves. © Atomic Spectroscopy Press Limited. All rights reserved.en_US
dc.identifier.endpage112en_US
dc.identifier.issn0195-5373
dc.identifier.issue3en_US
dc.identifier.scopus2-s2.0-85074898399
dc.identifier.scopusqualityQ2
dc.identifier.startpage104en_US
dc.identifier.urihttps://hdl.handle.net/11468/25148
dc.identifier.volume40en_US
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherAtomic Spectroscopy Press Limiteden_US
dc.relation.ispartofAtomic Spectroscopy
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.titleA new preconcentration method for the determination of pb and ni in real samples by using amberlite xad-16 functionalized with 1,6-bis(2-carboxy aldehyde phenoxy)butaneen_US
dc.titleA new preconcentration method for the determination of pb and ni in real samples by using amberlite xad-16 functionalized with 1,6-bis(2-carboxy aldehyde phenoxy)butane
dc.typeArticleen_US

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