Magnetic solid-phase extraction based on Coriolus versicolor-immobilized ? -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water
dc.contributor.author | Yalçın, Mustafa Serkan | |
dc.contributor.author | Özdemir, Sadin | |
dc.contributor.author | Soylak, Mustafa | |
dc.contributor.author | Kılınç, Ersin | |
dc.date.accessioned | 2024-04-24T19:11:39Z | |
dc.date.available | 2024-04-24T19:11:39Z | |
dc.date.issued | 2019 | |
dc.department | Dicle Üniversitesi | en_US |
dc.description.abstract | A method for preconcentration of Al(III) prior to its determination by inductively coupled plasma-opticalemission spectrometry (ICP-OES) was developed because the sensitivity of ICP-OES is insufficient for trace-level measurement of Al(III). The method is based on the use of Coriolus versicolor-immobilized ? -Fe 2 O3 magnetic nanoparticles as a solid phase sorbent. The best experimental conditions were found as pH 6.0, 2.0 mL/min flow rate, 100 mg amount of C. versicolor on 150 mg of ? -Fe 2 O3 nanoparticles, and 500 mL of sample volume. The Al(III) absorbed on biosorbent was eluted with 5.0 mL of 1.0 mol/L HCl. Limit of detection, limit of quantitation, linear range, correlation coefficient, relative standard deviation, and preconcentration factor were achieved as 0.03 ng/mL, 0.11 ng/mL, 0.2 to 20 ng/mL, 0.9994, 3%, and 100, respectively. Al(III) was preconcentrated in different water and food samples after successful results were achieved in the case of certified reference samples. | en_US |
dc.identifier.endpage | 1228 | en_US |
dc.identifier.issn | 1300-0527 | |
dc.identifier.issn | 1303-6130 | |
dc.identifier.issue | 5 | en_US |
dc.identifier.startpage | 1217 | en_US |
dc.identifier.uri | https://hdl.handle.net/11468/28131 | |
dc.identifier.volume | 43 | en_US |
dc.indekslendigikaynak | TR-Dizin | |
dc.language.iso | en | en_US |
dc.relation.ispartof | Turkish Journal of Chemistry | en_US |
dc.relation.publicationcategory | Makale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/openAccess | en_US |
dc.title | Magnetic solid-phase extraction based on Coriolus versicolor-immobilized ? -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water | en_US |
dc.type | Article | en_US |