Magnetic solid-phase extraction based on Coriolus versicolor-immobilized ? -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in water

dc.contributor.authorYalçın, Mustafa Serkan
dc.contributor.authorÖzdemir, Sadin
dc.contributor.authorSoylak, Mustafa
dc.contributor.authorKılınç, Ersin
dc.date.accessioned2024-04-24T19:11:39Z
dc.date.available2024-04-24T19:11:39Z
dc.date.issued2019
dc.departmentDicle Üniversitesien_US
dc.description.abstractA method for preconcentration of Al(III) prior to its determination by inductively coupled plasma-opticalemission spectrometry (ICP-OES) was developed because the sensitivity of ICP-OES is insufficient for trace-level measurement of Al(III). The method is based on the use of Coriolus versicolor-immobilized ? -Fe 2 O3 magnetic nanoparticles as a solid phase sorbent. The best experimental conditions were found as pH 6.0, 2.0 mL/min flow rate, 100 mg amount of C. versicolor on 150 mg of ? -Fe 2 O3 nanoparticles, and 500 mL of sample volume. The Al(III) absorbed on biosorbent was eluted with 5.0 mL of 1.0 mol/L HCl. Limit of detection, limit of quantitation, linear range, correlation coefficient, relative standard deviation, and preconcentration factor were achieved as 0.03 ng/mL, 0.11 ng/mL, 0.2 to 20 ng/mL, 0.9994, 3%, and 100, respectively. Al(III) was preconcentrated in different water and food samples after successful results were achieved in the case of certified reference samples.en_US
dc.identifier.endpage1228en_US
dc.identifier.issn1300-0527
dc.identifier.issn1303-6130
dc.identifier.issue5en_US
dc.identifier.startpage1217en_US
dc.identifier.urihttps://hdl.handle.net/11468/28131
dc.identifier.volume43en_US
dc.indekslendigikaynakTR-Dizin
dc.language.isoenen_US
dc.relation.ispartofTurkish Journal of Chemistryen_US
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.titleMagnetic solid-phase extraction based on Coriolus versicolor-immobilized ? -Fe2O3 nanoparticles for preconcentration and determination of Al(III) in wateren_US
dc.typeArticleen_US

Dosyalar