Crystal structure of a crown compound: (S)-2-isopropyl-N-benzyl-(benzo-monoaza-15-crown-5)

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dc.contributor.authorDoǧan, Nermin
dc.contributor.authorÖzbey, Süheyla
dc.contributor.authorTurgut, Yılmaz
dc.date.accessioned2024-04-24T17:56:52Z
dc.date.available2024-04-24T17:56:52Z
dc.date.issued2008
dc.departmentDicle Üniversitesi, Fen Fakültesi, Kimya Bölümüen_US
dc.description.abstractA new type of inclusion compound, (S)-2-isopropyl-N-benzyl-4,7,10,13-tetraoxa-8,9-benzo-1-azacyclopentadec-8-ene (1), has been prepared and studied by single-crystal X-ray diffraction techniques. The compound crystallizes in monoclinic space group C2 with cell dimensions a = 19.411(2), b = 6.1904(9), c = 19.780(2)Å, ? = 110.166(9)°, Z = 4. The crown ether oxygen atoms are nearly coplanar and the N1 atom deviates from the oxygen mean plane by -0.755 Å. The C-O and C-C distances of the 15-membered ring average 1.405(7) and 1.506(7)Å, while the O-C-C and C-O-C angles average 110.8(5) and 116.6(4)°. The N-C-C and C-N-C angles average 112.4(4)° and 115.1(4)°.en_US
dc.identifier.citationDoǧan, N., Özbey, S. ve Turgut, Y. (2008). Crystal structure of a crown compound: (S)-2-isopropyl-N-benzyl-(benzo-monoaza-15-crown-5). Analytical Sciences: X-ray Structure Analysis Online, 24(6), x107-x108.
dc.identifier.doi10.2116/analscix.24.x107
dc.identifier.endpagex108en_US
dc.identifier.issn1348-2238
dc.identifier.issue6en_US
dc.identifier.scopus2-s2.0-70450273410
dc.identifier.scopusqualityN/A
dc.identifier.startpagex107en_US
dc.identifier.urihttps://doi.org/10.2116/analscix.24.x107
dc.identifier.urihttps://hdl.handle.net/11468/23693
dc.identifier.volume24en_US
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherJapan Society for Analytical Chemistryen_US
dc.relation.ispartofAnalytical Sciences: X-ray Structure Analysis Online
dc.relation.publicationcategoryDiğeren_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.titleCrystal structure of a crown compound: (S)-2-isopropyl-N-benzyl-(benzo-monoaza-15-crown-5)en_US
dc.titleCrystal structure of a crown compound: (S)-2-isopropyl-N-benzyl-(benzo-monoaza-15-crown-5)
dc.typeNoteen_US

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