Browsing by Author "Ilhan, Salih"
Now showing items 1-19 of 19
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Prepared and characterization of new macrocyclic Schiff bases and their binuclear copper complexes
Temel, Hamdi; Ilhan, Salih (Pergamon-Elsevier Science Ltd, 2008)The new five macrocyclic ligands were synthesized by reaction of 2,6-diaminopyridine and various dialdehydes. Then, their copper(II) perchlorate complexes were synthesized by template effect by reaction of 2,6-diaminopyridine, ... -
Spectroscopic and electrochemical studies of transition metal complexes with N,N?-bis(2-aminothiophenol)-1,7-bis(2-formylphenyl)-1,4,7-trioxaheptane and structure effects on extractability of ligand towards some divalent cations
Temel, Hamdi; Alp, Hueseyin; Ilhan, Salih; Ziyadanogullari, Berrin; Yilmaz, Ismail (Springer Wien, 2007)La(III), Cu(II), Ni(II), and Zn(II) metal complexes with a novel quadridentate Schiff base derived from 1,7-bis(2-formylphenyl)-1,4,7-trioxaheptane and 2-aminothiophenol were synthesized and characterized by microanalytical ... -
Spectroscopic and extraction studies of new transition metal complexes with N,N'-bis(2-aminothiophenol)-1, 4-bis(2-carboxaldehydephenoxy)butane
Temel, Hamdi; Alp, Hueseyin; Ilhan, Salih; Ziyadanogullari, Berrin (Taylor & Francis Ltd, 2008)Metal complexes of La(III), Cu(II) and Ni(II) with a thio Schiff base derived from 1,4-bis(2-carboxaldehydephenoxy)butane and 2-aminothiophenol have been synthesized in absolute ethanol and characterized by microanalytical ... -
Synthesis and characterization of a new macrocyclic Schiff base derived from 2,6-diaminopyridine and 1,10-bis(2-formylphenyl)-1,4,7,10-tetraoxadecane and its Cu(II), Ni(II), Pb(II), Co(III) and La(III) complexes
Ilhan, Salih; Temel, Hamdi (Springer, 2007)A new macrocyclic ligand, 1,3,5-triaza-2,4:7,8:19,20-tribenzo-9,12,15,18-tetraoxacyclounkosa-1,5-diene (L) was synthesized by reaction of 2,6-diaminopyridine and 1,10-bis(2-formylphenyl)-1,4,7,10-tetraoxadecane. Then, its ... -
Synthesis and characterization of macrocyclic Cd(II) complexes
Ilhan, Salih; Temel, Hamdi (Natl Inst Science Communication-Niscair, 2008)Ten new Cd(II) complexes have been synthesized with Cd(ClO4)(2)center dot 6H(2)O, Cd(NO3)(2)center dot 6H(2)O in chloroform-methanol. The complexes have been characterized by elemental analysis, IR, H-1 NMR, UV-vis spectra, ... -
Synthesis and characterization of new macrocyclic Schiff base derived from 2,6-diaminopyridine and 1,7-bis(2-formylphenyl)-1,4,7-trioxaheptane and its Cu(II), Ni(II), Pb(II), Co(III) and La(III) complexes
Ilhan, Salih; Temel, Hamdi; Yilmaz, Ismail; Sekerci, Memet (Pergamon-Elsevier Science Ltd, 2007)A new macrocyclic ligand, 1,3,5-triaza-2,4:7,8:16,17-tribenzo-9,12,15-trioxacyclooktadeca-1,5-dien (L) was synthesized by reaction of 2,6-diaminopyridine and 1,7-bis(2-formylphenyl)-1,4,7-trioxaheptane. Then, its Cu(II), ... -
Synthesis and spectral characterization of macrocyclic NiII complexes derived from various diamines, NiII perchlorate and 1,4-bis(2-carboxyaldehydephenoxy)butane
Ilhan, Salih; Temel, Hamdi; Kilic, Ahmet; Tas, Esref (Springer, 2007)Six new macrocyclic complexes were synthesized by reaction of 1,4-bis(2-carboxyaldehyde phenoxy)butane with various diamines. Then, their nickel(II) perchlorate complexes were synthesized by the template effect by reaction ... -
Synthesis and spectral characterization of macrocyclic Schiff base by reaction of 2,6-diaminopyridine and 1,4-bis(2-carboxyaldehydephenoxy)butane and its CuII, NiII, PbII, CoIII and LaIII complexes
Ilhan, Salih; Temel, Hamdi; Ziyadanogullari, Recep; Sekerci, Memet (Springer, 2007)A new macrocyclic ligand, 1,3,5-triaza-2,4:7,8:15,16-tribenzo-9,15-dioxacycloheptadeca-1,5-diene (L) was synthesized by reaction of 2,6-diaminopyridine with 1,4-bis(2-carboxyaldehydephenoxy)butane. Then, its Cu-II, Ni-II, ... -
Synthesis and spectral studies of macrocyclic Cu(II) complexes by reaction of various diamines, copper(II) perchlorate and 1,4-bis(2-carboxyaldehyde phenoxy)butane
Ilhan, Salih; Temel, Hamdi; Kilic, Ahmet (Taylor & Francis Ltd, 2008)Six macrocyclic complexes, were synthesized by reaction of 1,4-bis(2-carboxyaldehyde phenoxy)butane and various amines and their copper(II) perchlorate complexes were synthesized by template effect reaction of 1,4-bis(2- ... -
Synthesis and spectral studies of macrocyclic Cu(II), Ni(II) and Co(II) complexes by template reaction of 1,4-bis(3-aminopropoxy)butane with metal(II) nitrate and salicylaldehyde derivatives
Ilhan, Salih; Temel, Hamdi (Elsevier, 2008)Six new macrocyclic complexes were synthesized by template reaction of salicylaldehyde derivatives with 1,4-bis(3-aminopropoxy)butane and metal(II) nitrate. The metal to ligand ratio of the complexes was found to be 1:1. ... -
Synthesis and Spectral Studies of Macrocyclic Pb(II), Zn(II), Cd(II) and La(III) Complexes by Template Reaction of 1,2-Bis(2-formylphenyl)ethane with Metal Nitrate and Various Diamine
Ilhan, Salih; Temel, Hamdi; Pasa, Salih; Tegin, Ibrahim (Maik Nauka/Interperiodica/Springer, 2010)Eight new macrocyclic complexes were synthesized by template reaction of 1,4-bis(3-aminopropoxy)butane or (+/-)-trans-1,2-diaminocyclohexane with metal nitrate and 1,2-bis(2-formylphenyl)ethane and their structures were ... -
Synthesis and spectroscopic characterization of a new macrocyclic Schiff base formed by the reaction of 1,5-bis(2-formylphenyl)pentane and 2,6-diaminopyridine, and a study of its metal complexes
Ilhan, Salih; Temel, Hamdi (Taylor & Francis Ltd, 2009)A new dialdehyde 1,5-bis(2-formylphenyl)pentane was synthesized from 1,5-dibromopentane with salicylaldehyde and K2CO3; macrocyclic ligand was synthesized by reaction of 2,6-diaminopyridine and 1,5-bis(2-formylphenyl) ... -
Synthesis and spectroscopic studies of novel transition metal complexes with schiff base synthesized from 1,4-bis-(o-aminophenoxy)butane and salicyldehyde
Temel, Hamdi; Ilhan, Salih (Maik Nauka/Interperiodica/Springer, 2009)The new Co(II), Cu(II), Ni(II) and Zn(II) complexes of potentially N2O2 Schiff base ligand [N,N'-bis(salicyldehydene)-1,4-bis-(o-aminophenoxy)butane] (H2L) prepared from 1,4-bis-(o-aminophenoxy)butane and salicyldehyde in ... -
Synthesis of complexes of Pb(II), Cd(II), Zn(II), Ni(II), La(III) and Cu(II) with a Schiff base macrocyclic ligand containing pyridine
Ilhan, Salih; Temel, Hamdi (Sage Publications Ltd, 2010)1,5-bis(2-formylphenyl)pentane (synthesised from 1,5 dibromopentane and salicylaldehyde). reacts with 2,6-diaminopyridine to give a new macrocyclic ligand that gives Cu(II), Ni(II), Pb(II), Zn(II), Cd(II) and La(III) ... -
Synthesis, characterization and electro-spectroelectrochemical studies of four macrocyclic Schiff-base Co(II) complexes having N2O2 set of donor atoms
Yilmaz, Ismail; Ilhan, Salih; Temel, Hamdi; Kilic, Ahmet (Springer, 2009)Four macrocyclic Schiff-base cobalt complexes, [CoL1][NO3](2) center dot A 3H(2)O, [CoL2][NO3](2) center dot A 4H(2)O, [CoL3][NO3](2) center dot A 4H(2)O and [CoL4][NO3](2) center dot A 2H(2)O, were synthesized by reaction ... -
Synthesis, characterization and redox properties of macrocyclic Schiff base by reaction of 2,6-diaminopyridine and 1,3-bis(2-carboxyaldehyde phenoxy) propane and its CuII, NiII, PbII, CoIII and LaIII complexes
Ilhan, Salih; Temel, Hamdi; Yilmaz, Ismail; Kilic, Ahmet (Springer, 2007)A new macrocyclic ligand, 1,3,5-triaza-2,4:7,8:, 14,15-tribenzo-9,13-dioxacyclohexadeca-1,5-diene ( L) was synthesized by reaction of 2,6-diaminopyridine and 1,3-bis(2-carboxyaldehyde phenoxy) propane. Then, its Cu-II, ... -
Synthesis, spectroscopic and electrochemical studies of novel transition metal complexes with N,N?-bis(2-hydroxynaphthalin-1-carbaldehydene)-1,3-bis-(o-aminophenoxy)propane
Temel, Hamdi; Ilhan, Salih; Aslanoglu, Mehmet; Alp, Huseyin (Natl Inst Science Communication, 2007)A novel Schiff base obtained by the reaction of 1,3-bis-(oaminophenoxy)propane and 2-hydroxynaphthalin-1-carbaldehyde, forms complexes with Co(II), Cu(II) and Ni(II). The Schiff base ligand and its metal complexes have ... -
Synthesis, structural characterization and electrochemical studies of new macrocyclic Schiff base containing pyridine head and its metal complexes
Ilhan, Salih; Temel, Hamdi; Yilmaz, Ismail; Sekerci, Memet (Elsevier Science Sa, 2007)A new macrocyclic ligand, 1,3,5-triaza-2,4:7,8:13,14-tribenzo-9,12-dioksa-cyclopentadeca-1,5-diene was synthesized by reaction of 2,6-diaminopyridine and 1,2-bis(2-carboxyaldehyde phenoxy)ethane. Then, its Cu(II), Ni(II), ... -
Synthesis, structural characterization of new macrocyclic Schiff base derived from 1,6-bis(2-formylphenyl)hexane and 2,6-diaminopyridine and its metal complexes
Ilhan, Salih; Ternel, Hamdi; Sunkur, Murat; Tegin, Ibrahim (Natl Inst Science Communication-Niscair, 2008)A macrocyclic ligand has been synthesized by reaction of 2,6-diaminopyridine and 1,6-bis(2-formylphenyl).hexane. Its complexes with Cu(II), Ni(II), Pb(II), Zn(II), Cd(II) and La(III) have been synthesized by the reaction ...
