Kaplan, ŞerefÖztürk, GülşenAzizoğlu, Sevil Ş.Toğrul, Mahmut2022-07-062022-07-062018Kaplan, Ş., Öztürk, G., Azizoğlu, S. Ş. ve Toğrul, M. (2018). Synthesis of chiral tripodal receptors under solvent-free conditions using microwave irradiation for investigation of anion and cation recognition properties. Arkivoc, 2018(7), 482-494.1551-7004https://www.arkat-usa.org/arkivoc-journal/browse-arkivoc/ark.5550190.p010.759https://hdl.handle.net/11468/10129Amide based chiral tripodal receptor derivatives were synthesized under microwave irradiation in quite high yields (76%- 84%) and they were characterized by IR and 1D, 2D, 1H- and 13C-NMR spectroscopies. The recognition properties of these tripodal receptors towards some anions and organic ammonium salts were investigated by 1H-NMR titration in DMSO-d6. The tripodal (S)-phenyl receptor demonstrated a highly significant enantiomeric selectivity towards the (S)-(-)-1-phenyletylammonium perchlorate (ERF= 91.74 S).eninfo:eu-repo/semantics/openAccessMolecular recognitionTripodal receptorsCation and anion recognitionMicrowaveNMR titrationArticle20187482494WOS:0004561875000422-s2.0-8506236816410.24820/ark.5550190.p010.759Q4Q3