Gümgüm, BBiricik, NBaysal, A2024-04-242024-04-2420001042-6507https://doi.org/10.1080/10426500008082392https://hdl.handle.net/11468/16879Microwave heating technique was applied to the preparation of dialkyl dithiophosphoric acids from the reaction of alcohol with phosphorus pentasulphide. A microwave oven (CEM-MDS 2000) was utilised to determine the preparation conditions For the best yield of dialkyl dithiophosphoric acids under atmospheric pressure at various times and power. Six different (C-4-C-9) chain-length of dialkyl dithiophosphoric acids were studied. All experiments were performed in an open Teflon (poly-tetrafluoroethylene) vessel. The results obtained showed that the reaction of dialkyl dithiophosphoric acids can be achieved more rapidly using microwave heating than using conventional procedures.eninfo:eu-repo/semantics/closedAccessDialkyl Dithiophosphoric AcidsMicrowave IrradiationSynthesisArticle167111116WOS:0001684491000112-s2.0-003434623210.1080/10426500008082392N/AN/A