Gümgüm, BBiricik, NBaysal, A2024-04-242024-04-2420021042-65071563-5325https://doi.org/10.1080/10426500214305https://hdl.handle.net/11468/16880Microwave heating technique was applied to the preparation of dialkyl dithiophosphoric acids from the reaction of alcohol with phosphorus pentasulphide. A microwave oven (CEM-MDS 2000) was utilized to determine the preparation conditions for the best yield of dialkyl dithiophosphoric acids under atmospheric pressure at various times and power Six different (C-4-C-9) chain-length of dialkyl dithiophosphoric acids were studied. All experiments were performed in an open Teflon (poly-tetrafluoroethylene) vessel. The results obtained showed that the reaction of dialkyl dithiophosphoric acids can be achieved more rapidly using microwave heating than using conventional procedures.eninfo:eu-repo/semantics/closedAccessDialkyl Dithiophosphoric AcidsMicrowave IrradiationSynthesisArticle1771025072512WOS:0001790755000312-s2.0-003681175610.1080/10426500214305Q4Q4