Resolution of (±)-?-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatography

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dc.contributor.authorYılmaz, Hayrullah
dc.contributor.authorTopal, Giray
dc.contributor.authorÇakmak, Reşit
dc.contributor.authorHoşgören, Halil
dc.contributor.orcid0000-0002-5275-6606
dc.contributor.orcid0000-0003-0401-7419
dc.contributor.orcid0000-0002-7056-3912
dc.date.accessioned2024-04-24T15:59:22Z
dc.date.available2024-04-24T15:59:22Z
dc.date.issued2010
dc.departmentDicle Üniversitesi, Ziya Gökalp Eğitim Fakültesi, Matematik ve Fen Bilimleri Eğitimi Bölümüen_US
dc.description.abstractIn this study, a new Pirkle-type chiral column stationary phase for resolution of beta-methylphenylethyl amine was described by using activated Sepharose 4B as a matrix, L-tyrosine as a spacer arm, and an aromatic amine derivative of L-glutamic acid as a ligand. The binding capacities of the stationary phase were determined at different pH values (pH = 6, 7, and 8) using buffer solutions as mobile phase, and enantiomeric excess (ee) was determined by HPLC equipped with chiral column. The ee was found to be 47%. Chirality 22:252-257, 2010. (C) 2009 Wiley-Liss, Inc.en_US
dc.description.sponsorshipTUBITAK (The Scientific and Technological Research Council of Turkey) [1061724 (TBAG-HD/224)]en_US
dc.description.sponsorshipContract grant sponsor: TUBITAK (The Scientific and Technological Research Council of Turkey); Contract grant number: 1061724 (TBAG-HD/224).en_US
dc.identifier.citationYılmaz, H., Topal, G., Çakmak, R. ve Hoşgören, H. (2010). Resolution of (±)-β-methylphenylethylamine by a novel chiral stationary phase for Pirkle-type column chromatography. Chirality, 22(2), 252-257.
dc.identifier.doi10.1002/chir.20736
dc.identifier.endpage257en_US
dc.identifier.issn0899-0042
dc.identifier.issn1520-636X
dc.identifier.issue2en_US
dc.identifier.pmid19496136
dc.identifier.scopus2-s2.0-74749084034
dc.identifier.scopusqualityQ2
dc.identifier.startpage252en_US
dc.identifier.urihttps://doi.org/10.1002/chir.20736
dc.identifier.urihttps://hdl.handle.net/11468/14011
dc.identifier.urihttps://onlinelibrary.wiley.com/doi/10.1002/chir.20736
dc.identifier.volume22en_US
dc.identifier.wosWOS:000273628300010
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofChirality
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSepharose 4ben_US
dc.subjectResolutionen_US
dc.subjectChiral aminesen_US
dc.subjectHplcen_US
dc.subjectPirkle-type column chromatographyen_US
dc.titleResolution of (±)-?-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatographyen_US
dc.titleResolution of (±)-?-Methylphenylethylamine by a Novel Chiral Stationary Phase for Pirkle-Type Column Chromatography
dc.typeArticleen_US

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