Comparison of Cd(II) preconcentrations by using magnetized Pleurotus erygnii and Coprinus micaceus and its determination in real samples

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dc.contributor.authorOzdemir, Sadin
dc.contributor.authorYalcin, M. Serkan
dc.contributor.authorKilinc, Ersin
dc.contributor.authorSoylak, Mustafa
dc.date.accessioned2024-04-24T16:15:30Z
dc.date.available2024-04-24T16:15:30Z
dc.date.issued2019
dc.departmentDicle Üniversitesien_US
dc.description.abstractThe utilization of the magnetized Pleurotus erygnii and Coprinus micaceus with gamma-Fe2O3 nanoparticles as biosorbents for magnetic solid phase extraction (MSPE) of Cd(II) were investigated in details. The surface structures of magnetized P. erygnii and C. micaceus were investigated by the Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscope (SEM) and energy dispersive X-ray (EDX). The best process conditions were tested and determined as pH 5, 3 mL min(-1) flow rate, 100 mg of P. erygnii and C. micaceus on 75 mg of gamma-Fe2O3 nanoparticles, 5 mL of 1 mol L-1 HCl as eluent, and 400 mL of sample volume for both biosorbents. The limit of detections (LOD) were achieved as 0.054 ng mL(-1) and 0.040 ng(-1) for magnetized P. erygnii and C. micaceus, respectively. Preconcentration factors were determined as 80 for both magnetized biosorbents. The recommended methods were validated using certificated reference materials. Cd(II) in different real samples were determined by ICP-OES (inductively coupled plasma optical emission spectrometry) after preconcentration with developed methods.en_US
dc.identifier.doi10.1016/j.microc.2018.08.039
dc.identifier.endpage25en_US
dc.identifier.issn0026-265X
dc.identifier.issn1095-9149
dc.identifier.scopus2-s2.0-85052451770
dc.identifier.scopusqualityQ1
dc.identifier.startpage19en_US
dc.identifier.urihttps://doi.org/10.1016/j.microc.2018.08.039
dc.identifier.urihttps://hdl.handle.net/11468/15831
dc.identifier.volume144en_US
dc.identifier.wosWOS:000449893000004
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherElsevier Science Bven_US
dc.relation.ispartofMicrochemical Journal
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectPleurotus Erygniien_US
dc.subjectCoprinus Micaceusen_US
dc.subjectGamma-Fe2o3 Nanoparticleen_US
dc.subjectMagnetic Solid Phase Extractionen_US
dc.subjectPreconcentrationen_US
dc.subjectCden_US
dc.titleComparison of Cd(II) preconcentrations by using magnetized Pleurotus erygnii and Coprinus micaceus and its determination in real samplesen_US
dc.titleComparison of Cd(II) preconcentrations by using magnetized Pleurotus erygnii and Coprinus micaceus and its determination in real samples
dc.typeArticleen_US

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