Supramolecular solvent-based-vortex-assisted-dispersive liquid liquid microextraction of Sudan Black B in food samples prior to spectrophotometric detection
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Tarih
2024
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Tubitak Scientific & Technological Research Council Turkey
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
A new, simple and rapid spectrophotometric method was developed for determination of Sudan Black B in food products by supramolecular solvent -based -vortex -assisted -dispersive liquid liquid microextraction (SUPRAS-VA-DLLME). Extraction solvent type, volume of solvent, pH, volume of THF, centrifugation time, vortex time, and sample volume were investigated as optimization parameters of the developed method. Under the optimum conditions, limit of detection and limit of quantification, preconcentration factor and enhancement factor of the developed method were calculated to be 9.01 mu g L -1 , 29.73 mu g L -1 , 20, and 55, respectively. The developed microextraction method was successfully applied to food samples for the determination of Sudan Black B.
Açıklama
Anahtar Kelimeler
Preconcentration, spectrophotometric determination, Sudan Black B, supramolecular solvent, dispersive liquid liquid microextraction
Kaynak
Turkish Journal of Chemistry
WoS Q Değeri
Q3
Scopus Q Değeri
Q3
Cilt
48
Sayı
2
